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RMS Annual Session combined with the Fedorov Session 2012
Saint Petersburg, Russia
8-10 October 2012
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Synthesis and crystal structure of the new potassium uranyl selenate K5[(UO2)4(SeO4)6(H2O)2](NO3)(H2O)8

RMS-DPI code:  2012-1-150-0
Scientific session:  F1. Mineralogical crystallogrpaphy and crystal chemistry
Author listing:  Gurzhiy V.V., Tyumentseva O.S., Krivovichev S.V.
Principal author:  Gurzhiy Vladislav Vladimirovich
Language:  Russian
Abstract - Summary 
(short description):
Single crystals of K5[(UO2)4(SeO4)6(H2O)2](NO3)(H2O)8 (1) were prepared by evaporation from 2 ml aqueous solution of uranyl nitrate, potassium carbonate and selenic acid. Compound 1 has a monoclinic symmetry, space group C2/c, a = 20.290(4) Å, b = 10.380(2) Å, c = 21.436(4) Å, V = 103.446(3) o, V = 4391.0(13) Å3. The crystal structure was solved by direct methods from X-ray diffraction data and refined by the least-squares method to R1 = 0.027 (wR2 = 0.066) for 6405 reflections with |Fo| ≥ 4σF.
 
Date of presentation:  09/10/2012
Presentation Place:  Mining University, foyer of the Assembly Hall
 
RMS-DPI code:  2012-1-150-0
Proceeedings volume 
in the RMS catalogue:
 
Mineralogy in а whole space of the word.
File of proceedings 
(PDF): 
 218 K
Status:  printed
Accepted:  28/08/2012
Published on-line:  05/11/2012
Permanent address of publication:  http://www.minsoc.ru/2012-1-150-0/
Contact author(s):  Gurzhiy, Vladislav Vladimirovich
 

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